3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Base Information

Chemical Name:3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole
CAS No.:1609394-06-0
Molecular Formula:C₁₅H₂₂N₄O₄Si
Molecular Weight:350.45
Hs Code.:

Synonyms:3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

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Chemical Property of 3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

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Technology Process of 3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

There total 5 articles about 3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1609394-05-9
3-(2-methoxy-3-nitrophenyl)-4H-1,2,4-triazole

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1609394-06-0
3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 - 25 ℃; for 3h;

Reference yield:

: 22621-41-6
2-hydroxy-3-nitro-benzoic acid methyl ester

: 1609394-06-0
3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 - 60 °C

2.1: ammonium hydroxide; ammonia / water; methanol / 20 - 25 °C / Sealed tube

3.1: 0.5 h / 95 °C

3.2: 4 h / 20 - 25 °C / Cooling with ice

4.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 3 h / 20 - 25 °C

With dmap; ammonium hydroxide; ammonia; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 90564-26-4
2-methoxy-3-nitro-benzoic acid methyl ester

: 1609394-06-0
3-(2-methoxy-3-nitrophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium hydroxide; ammonia / water; methanol / 20 - 25 °C / Sealed tube

2.1: 0.5 h / 95 °C

2.2: 4 h / 20 - 25 °C / Cooling with ice

3.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 3 h / 20 - 25 °C

With dmap; ammonium hydroxide; ammonia; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; water;