[2-bis(trimethylsilyl)methyl-5-dimethylamino-3-phenyl-2H-1,4,2-diazaphosphole-κP]pentacarbonylmolybdenum(0)

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Chemical Name:[2-bis(trimethylsilyl)methyl-5-dimethylamino-3-phenyl-2H-1,4,2-diazaphosphole-κP]pentacarbonylmolybdenum(0)
CAS No.:1313434-04-6
Molecular Formula:C₂₂H₃₀MoN₃O₅PSi₂
Molecular Weight:599.582
Hs Code.:

Synonyms:[2-bis(trimethylsilyl)methyl-5-dimethylamino-3-phenyl-2H-1,4,2-diazaphosphole-κP]pentacarbonylmolybdenum(0)

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Chemical Property of [2-bis(trimethylsilyl)methyl-5-dimethylamino-3-phenyl-2H-1,4,2-diazaphosphole-κP]pentacarbonylmolybdenum(0)

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Technology Process of [2-bis(trimethylsilyl)methyl-5-dimethylamino-3-phenyl-2H-1,4,2-diazaphosphole-κP]pentacarbonylmolybdenum(0)

There total 1 articles about [2-bis(trimethylsilyl)methyl-5-dimethylamino-3-phenyl-2H-1,4,2-diazaphosphole-κP]pentacarbonylmolybdenum(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 207723-64-6
pentacarbonyl[2-(bis(trimethylsilyl)methyl)-3-phenyl-2H-azaphosphirene-κP]molybdenum(0)

: 1493-13-6
trifluorormethanesulfonic acid

: 1467-79-4
NCNMe₂

: 1313434-04-6
[2-bis(trimethylsilyl)methyl-5-dimethylamino-3-phenyl-2H-1,4,2-diazaphosphole-κP]pentacarbonylmolybdenum(0)

Guidance literature:: With N(C₂H₅)3; In dichloromethane; byproducts: [(C2H5)3NH][CF3SO3]; (Ar, Schlenk technique); addn. of dimethylcyanamide and then triflic acid to CH2Cl2 soln. of molybdenum compd. at -30°C, keeping for 2 min, addn. of triethylamine; evapn., chromy. (silica, petroleum ether/diethyl ether (100:1)) at -30°C, evapn., elem. anal.;
DOI:10.1016/j.poly.2011.04.014