C₆H₅C(NOH)C(NO)C₆H₅Sn(CH₂CH₂CH₂CH₃)3

Base Information

• Chemical Name: C₆H₅C(NOH)C(NO)C₆H₅Sn(CH₂CH₂CH₂CH₃)3
• CAS No.: 256524-18-2
• Molecular Formula: C₂₆H₃₈N₂O₂Sn
• Molecular Weight: 529.31
• Mol file: 256524-18-2.mol

Synonyms:C₆H₅C(NOH)C(NO)C₆H₅Sn(CH₂CH₂CH₂CH₃)3

Chemical Property of C₆H₅C(NOH)C(NO)C₆H₅Sn(CH₂CH₂CH₂CH₃)3

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₆H₅C(NOH)C(NO)C₆H₅Sn(CH₂CH₂CH₂CH₃)3

There total 1 articles about C₆H₅C(NOH)C(NO)C₆H₅Sn(CH₂CH₂CH₂CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

tributyltin chloride (1461-22-9) + sodium (7440-23-5) + benzildioxime (23873-81-6) → C6H5C(NOH)C(NO)C6H5Sn(CH2CH2CH2CH3)3 (256524-18-2) + sodium chloride (7647-14-5)

Guidance literature:

In isopropyl alcohol; benzene; strictly anhydrous conditions; addn. of Na to excess of i-PrOH, refluxing (0.5 h), cooling, addn. of oxime, refluxing (2 h), cooling, addn. of stoichiom. amt. of Sn compound in benzene, refluxing (2 h); sovent removal (reduced pressure), filtration off of NaCl, crystn. (benzene/petroleum ether); elem. anal.;

DOI:10.1080/00945719909351730

upstream raw materials:

tributyltin chloride

sodium

benzildioxime

Refernces