1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride

Base Information

• Chemical Name: 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride
• CAS No.: 75995-63-0
• Molecular Formula: C₂₂H₂₈N₂O₃*ClH
• Molecular Weight: 404.937

Synonyms:1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride

Chemical Property of 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride

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Technology Process of 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride

There total 2 articles about 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one (75995-62-9) → 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride (75995-63-0)

Guidance literature:

With silica gel; at 100 ℃; for 0.5h;

Reference yield: 31.0%

N-benzyl-α-bromoisobutyranilide (60110-37-4) → 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride (75995-63-0) + 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one (75995-62-9)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield: 92.0%

1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride (75995-63-0) → 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate (75995-64-1)

Guidance literature:

With sodium hydrogencarbonate; In chloroform;

upstream raw materials:

N-benzyl-α-bromoisobutyranilide

2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one

Downstream raw materials:

1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate

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