2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one

Base Information

• Chemical Name: 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one
• CAS No.: 75995-62-9
• Molecular Formula: C₂₂H₂₇BrN₂O₂
• Molecular Weight: 431.373

Synonyms:2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one

Chemical Property of 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one

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Technology Process of 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one

There total 4 articles about 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

N-benzyl-α-bromoisobutyranilide (60110-37-4) → 1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride (75995-63-0) + 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one (75995-62-9)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

2-pyrrolidinon (616-45-5) + N-benzyl-α-bromoisobutyranilide (60110-37-4) → N-benzylmethacrylamide (3219-55-4) + 4-benzyl-2,2-dimetyl-1-oxa-4,6-diazaspiro<4,4>nonan-3-one (115539-43-0) + 3-Benzyl-2-benzylamino-2-isopropenyl-5,5-dimethyl-oxazolidin-4-one (78877-71-1) + 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one (75995-62-9)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, RT, 2.) THF, 1.5 h;

Reference yield:

piperidin-2-one (675-20-7) + N-benzyl-α-bromoisobutyranilide (60110-37-4) → N-benzylmethacrylamide (3219-55-4) + 4-benzyl-2,2-dimethyl-1-oxa-4,6-diazaspiro<4,5>decan-3-one (115539-44-1) + 3-Benzyl-2-benzylamino-2-isopropenyl-5,5-dimethyl-oxazolidin-4-one (78877-71-1) + 2-benzylamino-2-(1-bromoisopropyl)-3-benzyl-5,5-dimethyloxazolidin-4-one (75995-62-9)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, 50 deg C, 2.) THF, 1.5 h;

upstream raw materials:

2-pyrrolidinon

N-benzyl-α-bromoisobutyranilide

piperidin-2-one

caprolactam

Downstream raw materials:

1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate

1-benzylcarbamoyl-1-methylethyl 2-benzylaminoisobutyrate hydrochloride

benzylamine hydrochloride

1-benzylcarbamoyl-1-methylethyl 2-bromoisobutyrate

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