N₅-(2-aminoethylcarbonyl)-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

Base Information

• Chemical Name: N₅-(2-aminoethylcarbonyl)-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene
• CAS No.: 1166232-46-7
• Molecular Formula: C₃₄H₃₂N₄O₃
• Molecular Weight: 544.653

Synonyms:N₅-(2-aminoethylcarbonyl)-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

Chemical Property of N₅-(2-aminoethylcarbonyl)-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

Chemical Property:

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Technology Process of N₅-(2-aminoethylcarbonyl)-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

There total 1 articles about N₅-(2-aminoethylcarbonyl)-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N5-[2-(trifluoroacetylamino)ethylcarbonyl]-N1-(tritylaminooxyacetyl)-1,5-diaminonaphthalene (1166232-45-6) → N5-(2-aminoethylcarbonyl)-N1-(tritylaminooxyacetyl)-1,5-diaminonaphthalene (1166232-46-7)

Guidance literature:

With ammonium hydroxide; In ethanol; at 60 ℃; for 4h;

DOI:10.1021/ja904767k

Reference yield: 94.0%

N5-(2-aminoethylcarbonyl)-N1-(tritylaminooxyacetyl)-1,5-diaminonaphthalene (1166232-46-7) + 9-fluorenylmethoxycarbonyl isothiocyanate (199915-38-3) → N5-[2-(N3-fluorenylmethyloxycarbonylthioureido)ethylcarbonyl]-N1-(tritylaminooxyacetyl)-1,5-diaminonaphthalene (1166232-53-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile; at 20 ℃;

DOI:10.1021/ja904767k

Reference yield:

N5-(2-aminoethylcarbonyl)-N1-(tritylaminooxyacetyl)-1,5-diaminonaphthalene (1166232-46-7) + 1H-pyrazole-1-carboximidamide hydrochloride (4023-02-3) → N5-(2-guanidinoethylcarbonyl)-N1-(tritylaminooxyacetyl)-1,5-diaminonaphthalene (1166232-48-9)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

DOI:10.1021/ja904767k

upstream raw materials:

N₅-[2-(trifluoroacetylamino)ethylcarbonyl]-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

Downstream raw materials:

N₅-(2-guanidinoethylcarbonyl)-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

N₅-[2-(N₃-fluorenylmethyloxycarbonylthioureido)ethylcarbonyl]-N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

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