2-methoxy-4-methylisovalerophenone

Base Information

Chemical Name:2-methoxy-4-methylisovalerophenone
CAS No.:71898-88-9
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:2-methoxy-4-methylisovalerophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methoxy-4-methylisovalerophenone

Chemical Property:

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Technology Process of 2-methoxy-4-methylisovalerophenone

There total 4 articles about 2-methoxy-4-methylisovalerophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.1%

: 105337-38-0
1-(2-hydroxy-4-methyl-phenyl)-3-methyl-butan-1-one

: 77-78-1
dimethyl sulfate

: 71898-88-9
2-methoxy-4-methylisovalerophenone

Guidance literature:: With potassium carbonate; In acetone; for 10h; Heating;
DOI:10.1246/bcsj.62.2102

Reference yield:

: 105401-73-8
3-methylphenyl 3-methylbutyrate

: 71898-88-9
2-methoxy-4-methylisovalerophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 95.3 percent / AlCl₃ / CS₂ / 1.) reflux, 2 h, 2.) 145 to 150 deg C, 4 h

2: 96.1 percent / K₂CO₃ / acetone / 10 h / Heating

With aluminium trichloride; potassium carbonate; In carbon disulfide; acetone;
DOI:10.1246/bcsj.62.2102

Reference yield:

: 108-39-4
3-methyl-phenol

: 71898-88-9
2-methoxy-4-methylisovalerophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 94.7 percent / benzene / 1 h / Heating

2: 95.3 percent / AlCl₃ / CS₂ / 1.) reflux, 2 h, 2.) 145 to 150 deg C, 4 h

3: 96.1 percent / K₂CO₃ / acetone / 10 h / Heating

With aluminium trichloride; potassium carbonate; In carbon disulfide; acetone; benzene;
DOI:10.1246/bcsj.62.2102