3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde

Base Information

Chemical Name:3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde
CAS No.:1228585-85-0
Molecular Formula:C₁₈H₂₁N₅O₃
Molecular Weight:355.396
Hs Code.:

Synonyms:3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde

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Chemical Property of 3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde

Chemical Property:

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Technology Process of 3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde

There total 5 articles about 3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228585-84-9
3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzonitrile

: 1228585-85-0
3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde

Guidance literature:: With formic acid; Raney nickel; at 80 ℃; for 1.5h;

Reference yield:

: ((2-ethoxy-2-oxoethylamino)methyl)benzonitrile

: 1228585-85-0
3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonia / tetrahydrofuran; methanol / 1 h / 0 °C / Inert atmosphere

1.2: 16 h / 20 °C / Inert atmosphere

2.1: peracetic acid / acetonitrile / 2 h / Inert atmosphere; Cooling with ice

3.1: trifluoroacetic acid / 100 °C

4.1: hydrogen; palladium on activated charcoal / ethanol; acetonitrile / 18 h

5.1: nickel; formic acid / 1.5 h / 80 °C

With peracetic acid; formic acid; palladium on activated charcoal; ammonia; hydrogen; nickel; trifluoroacetic acid; In tetrahydrofuran; methanol; ethanol; acetonitrile;
DOI:10.1021/jm400815m

Reference yield:

: C₁₇H₁₈N₆O₆S

: 1228585-85-0
3-((4-amino-2-butoxy-6-oxo-6,7-dihydropteridin-8(5H)-yl)methyl)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / 100 °C

2: hydrogen; palladium on activated charcoal / ethanol; acetonitrile / 18 h

3: nickel; formic acid / 1.5 h / 80 °C

With formic acid; palladium on activated charcoal; hydrogen; nickel; trifluoroacetic acid; In ethanol; acetonitrile;
DOI:10.1021/jm400815m