phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate

Base Information

Chemical Name:phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate
CAS No.:1419604-52-6
Molecular Formula:C₂₀H₂₈N₂O₃Si
Molecular Weight:372.539
Hs Code.:

Synonyms:phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate

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Chemical Property of phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate

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Technology Process of phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate

There total 5 articles about phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1419604-50-4
6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-amine

: 1885-14-9
phenyl chloroformate

: 1419604-52-6
phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate

Guidance literature:: With pyridine; In acetone; at 0 ℃; for 4h;

Reference yield:

: 13603-40-2
(6-methyl-5-nitropyridin-2-yl)methanol

: 1419604-52-6
phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / dichloromethane / 1 h / 0 °C

2: hydrogen; palladium on activated charcoal / methanol / 16 h / 2068.65 Torr

3: pyridine / acetone / 4 h / 0 °C

With pyridine; 1H-imidazole; palladium on activated charcoal; hydrogen; In methanol; dichloromethane; acetone;

Reference yield:

: 15513-52-7,767567-84-0
3-nitro-2,6-lutidine

: 1419604-52-6
phenyl 6-((tert-butyldimethylsilyloxy)methyl)-2-methylpyridin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: selenium(IV) oxide / 1,4-dioxane / 16 h / 100 °C

2: sodium tetrahydroborate; methanol / 1 h / 0 °C

3: 1H-imidazole / dichloromethane / 1 h / 0 °C

4: hydrogen; palladium on activated charcoal / methanol / 16 h / 2068.65 Torr

5: pyridine / acetone / 4 h / 0 °C

With pyridine; 1H-imidazole; methanol; selenium(IV) oxide; sodium tetrahydroborate; palladium on activated charcoal; hydrogen; In 1,4-dioxane; methanol; dichloromethane; acetone;