2-cyclohexen-1-one, 5,5-dimethyl-3-[(5-methyl-3-isoxazolyl

Base Information

• Chemical Name: 2-cyclohexen-1-one, 5,5-dimethyl-3-[(5-methyl-3-isoxazolyl
• CAS No.: 897660-79-6
• Molecular Formula: C₁₂H₁₆N₂O₂
• Molecular Weight: 220.271
• Mol file: 897660-79-6.mol

Synonyms:3-((5-methylisoxazol-3-yl)amino)-5,5-dimethylcyclohex-2-enone

Chemical Property of 2-cyclohexen-1-one, 5,5-dimethyl-3-[(5-methyl-3-isoxazolyl

Chemical Property:

Purity/Quality:

5,5-Dimethyl-3-[(5-methylisoxazol-3-yl)amino]-cyclohex-2-en-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of 2-cyclohexen-1-one, 5,5-dimethyl-3-[(5-methyl-3-isoxazolyl

There total 1 articles about 2-cyclohexen-1-one, 5,5-dimethyl-3-[(5-methyl-3-isoxazolyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.4%

5-methylisoxazol-3-ylamine (1072-67-9) + dimedone (3471-13-4) → 3-((5-methylisoxazol-3-yl)amino)-5,5-dimethylcyclohex-2-enone (897660-79-6)

Guidance literature:

In ethanol; ethyl acetate; for 6h; Reflux;

DOI:10.1016/j.ejmech.2012.02.003

Reference yield: 92.0%

3-((5-methylisoxazol-3-yl)amino)-5,5-dimethylcyclohex-2-enone (897660-79-6) + 2,2-dihydroxy-1-phenyl-ethanone (1075-06-5) + 5-[(E)-2-(4-Chloro-phenyl)-vinyl]-3-methyl-isoxazol-4-ylamine (754985-41-6) → (E)-3-((5-(4-chlorostyryl)-3-methylisoxazol-4-yl)amino)-6,6-dimethyl-1-(5-methylisoxazol-3-yl)-2-phenyl-6,7-dihydro-1H-indol-4(5H)-one

Guidance literature:

With acetic acid; In water; at 100 ℃; for 1h; Reflux; Green chemistry;

DOI:10.1016/j.tetlet.2017.11.027

Reference yield: 92.0%

(E)-4-amino-3-methyl-5-styrylisoxazole (51978-96-2) + 3-((5-methylisoxazol-3-yl)amino)-5,5-dimethylcyclohex-2-enone (897660-79-6) + 1-(4-bromophenyl)-2,2-dihydroxyethanone (80352-42-7) → (E)-2-(4-bromophenyl)-6,6-dimethyl-3-((3-methyl-5-styrylisoxazol-4-yl)amino)-1-(5-methylisoxazol-3-yl)-6,7-dihydro-1H-indol-4(5H)-one

Guidance literature:

With acetic acid; In water; at 100 ℃; for 1h; Reflux; Green chemistry;

DOI:10.1016/j.tetlet.2017.11.027

upstream raw materials:

5-methylisoxazol-3-ylamine

dimedone

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