(S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:(S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole
CAS No.:1443650-82-5
Molecular Formula:C₁₉H₂₀N₈O₂S₂
Molecular Weight:456.552
Hs Code.:

Synonyms:(S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole

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Technology Process of (S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole

There total 4 articles about (S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1443650-81-4
(2S)-2-methyl-4-(1-phenyl-1H-tetrazole-5-sulfonyl)butan-1-ol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1443650-82-5
(S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201204545

Reference yield:

: 70423-38-0
(S)-2-methyl-1,4-butandiol

: 1443650-82-5
(S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / -78 - 20 °C / Inert atmosphere

2: ammonium molybdate; dihydrogen peroxide / ethanol / 16 h / 0 - 20 °C / Inert atmosphere

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

With ammonium molybdate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol; 1: |Mitsunobu Displacement / 3: |Mitsunobu Displacement;
DOI:10.1002/chem.201204545

Reference yield:

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1443650-82-5
(S)-5-(2-methyl-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butylthio)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / -78 - 20 °C / Inert atmosphere

2: ammonium molybdate; dihydrogen peroxide / ethanol / 16 h / 0 - 20 °C / Inert atmosphere

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

With ammonium molybdate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol; 1: |Mitsunobu Displacement / 3: |Mitsunobu Displacement;
DOI:10.1002/chem.201204545