O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate

Base Information

Chemical Name:O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate
CAS No.:904702-54-1
Molecular Formula:C₁₈H₁₉ClNO₈P
Molecular Weight:443.778
Hs Code.:

Synonyms:O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate

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Chemical Property of O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate

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Technology Process of O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate

There total 4 articles about O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 39784-11-7
(4-chloro-3-methylphenoxy)-acetyl chloride

: 103796-61-8
dimethyl 1-hydroxy-1-(3-nitrophenyl)methylphosphonate

: 904702-54-1
O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate

Guidance literature:: With pyridine; In chloroform; at 10 - 42 ℃;
DOI:10.1021/jf104247w

Reference yield:

: 59-50-7
4-Chloro-3-methylphenol

: 904702-54-1
O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide

2: thionyl chloride

3: pyridine / chloroform / 10 - 42 °C

With pyridine; thionyl chloride; sodium hydroxide; In chloroform;
DOI:10.1021/jf104247w

Reference yield:

: 588-20-5
4-chloro-3-methylphenoxyacetic acid

: 904702-54-1
O,O-dimethyl α-(3-methyl-4-chlorophenoxyacetoxy)-3-nitrobenzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: pyridine / chloroform / 10 - 42 °C

With pyridine; thionyl chloride; In chloroform;
DOI:10.1021/jf104247w