(4-methyl-2-(sec-phenethyl)phenyl)NCMe(C₅H₃N)CMeN(4-methyl-2-(sec-phenethyl)phenyl)

Base Information

• Chemical Name: (4-methyl-2-(sec-phenethyl)phenyl)NCMe(C₅H₃N)CMeN(4-methyl-2-(sec-phenethyl)phenyl)
• CAS No.: 1152309-77-7
• Molecular Formula: C₃₉H₃₉N₃
• Molecular Weight: 549.759

Synonyms:(4-methyl-2-(sec-phenethyl)phenyl)NCMe(C₅H₃N)CMeN(4-methyl-2-(sec-phenethyl)phenyl)

Chemical Property of (4-methyl-2-(sec-phenethyl)phenyl)NCMe(C₅H₃N)CMeN(4-methyl-2-(sec-phenethyl)phenyl)

Chemical Property:

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Technology Process of (4-methyl-2-(sec-phenethyl)phenyl)NCMe(C₅H₃N)CMeN(4-methyl-2-(sec-phenethyl)phenyl)

There total 1 articles about (4-methyl-2-(sec-phenethyl)phenyl)NCMe(C₅H₃N)CMeN(4-methyl-2-(sec-phenethyl)phenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

2,6-Diacetylpyridine (1129-30-2) + rac-4-methyl-2-sec-phenethylaniline (70660-38-7) → (4-methyl-2-(sec-phenethyl)phenyl)NCMe(C5H3N)CMeN(4-methyl-2-(sec-phenethyl)phenyl) (1152309-77-7)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 80 - 110 ℃; for 24h; Molecular sieve;

DOI:10.1021/om9010356

Reference yield: 84.0%

iron(II) chloride tetrahydrate + (4-methyl-2-(sec-phenethyl)phenyl)NCMe(C5H3N)CMeN(4-methyl-2-(sec-phenethyl)phenyl) (1152309-77-7) → [FeCl2((4-methyl-2-(sec-phenethyl)phenyl)NCMe(C5H3N)CMeN(4-methyl-2-(sec-phenethyl)phenyl))] (1152309-78-8)

Guidance literature:

In tetrahydrofuran; (N2); using Schlenk techniques; addn. of (C(CH3)NC6H3(CH3)C(CH3)C6H5)2C5H3N. to soln. of FeCl2*4H2O in THF at room temp. with violent stirring, pptn. for several minutes, stirring for 8 h at room temp.; removal of the supernatant liquid, washing 3 times with Et2O and drying under vac.; elem. anal.;

DOI:10.1021/om9010356

upstream raw materials:

2,6-Diacetylpyridine

rac-4-methyl-2-sec-phenethylaniline

Downstream raw materials:

[FeCl₂((4-methyl-2-(sec-phenethyl)phenyl)NCMe(C₅H₃N)CMeN(4-methyl-2-(sec-phenethyl)phenyl))]

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