tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester

Base Information

Chemical Name:tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester
CAS No.:256341-03-4
Molecular Formula:C₄₉H₈₀O₈
Molecular Weight:797.169
Hs Code.:

Synonyms:tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester

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Chemical Property of tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester

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Technology Process of tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester

There total 3 articles about tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 112-64-1
tetradecanoyl chloride

: 256341-02-3
2,2-bis[{(4-methoxybenzyl)oxy}methyl]propane-1,3-diol

: 256341-03-4
tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1016/S0040-4039(99)01934-6

Reference yield:

: 1130782-84-1,1130782-85-2
3,9-di(4-methoxyphenyl)-2,4,8,10-tetraoxaspiro<5,5>undecane

: 256341-03-4
tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DIBAL-H / hexane; CH₂Cl₂ / 22 h / 0 - 20 °C

2: 86 percent / Et₃N; DMAP / CH₂Cl₂ / 4 h / 0 - 20 °C

With dmap; diisobutylaluminium hydride; triethylamine; In hexane; dichloromethane; 1: Hydrogenation / 2: Esterification;
DOI:10.1016/S0040-4039(99)01934-6

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 256341-03-4
tetradecanoic acid 3-(4-methoxy-benzyloxy)-2-(4-methoxy-benzyloxymethyl)-2-tetradecanoyloxymethyl-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / TsOH / benzene / 12 h / Heating

2: 80 percent / DIBAL-H / hexane; CH₂Cl₂ / 22 h / 0 - 20 °C

3: 86 percent / Et₃N; DMAP / CH₂Cl₂ / 4 h / 0 - 20 °C

With dmap; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; In hexane; dichloromethane; benzene; 1: acetal formation / 2: Hydrogenation / 3: Esterification;
DOI:10.1016/S0040-4039(99)01934-6