1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate

Base Information

Chemical Name:1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate
CAS No.:871339-59-2
Molecular Formula:C₂₃H₃₀N₂O₃
Molecular Weight:382.503
Hs Code.:

Synonyms:1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate

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Chemical Property of 1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate

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Technology Process of 1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate

There total 5 articles about 1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 871339-58-1
1-(3-(benzyloxy)-2-methylphenyl)piperazine

: 24424-99-5
di-tert-butyl dicarbonate

: 871339-59-2
1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 30h;

Reference yield:

: 65361-82-2
3-benzyloxy-2-methyl-phenylamine

: 871339-59-2
1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / diethylene glycol dimethyl ether / 4 h / Heating / reflux

2: tetrahydrofuran / 30 h / 20 °C

With potassium carbonate; In tetrahydrofuran; diethylene glycol dimethyl ether;

Reference yield:

: 100-39-0
benzyl bromide

: 871339-59-2
1,1-dimethylethyl 4-{2-methyl-3-[(phenylmethyl)oxy]phenyl}piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

2.1: tin(ll) chloride / ethyl acetate / 5 h / 70 °C

2.2: 20 °C / pH 8

3.1: potassium carbonate / diethylene glycol dimethyl ether / 4 h / Heating / reflux

4.1: tetrahydrofuran / 30 h / 20 °C

With potassium carbonate; caesium carbonate; tin(ll) chloride; In tetrahydrofuran; diethylene glycol dimethyl ether; ethyl acetate; N,N-dimethyl-formamide;