tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate

Base Information

Chemical Name:tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate
CAS No.:1428526-86-6
Molecular Formula:C₂₃H₃₂NO₄P
Molecular Weight:417.485
Hs Code.:

Synonyms:tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate

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Chemical Property of tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate

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Technology Process of tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate

There total 8 articles about tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428526-85-5
tert-butyl N-((4-(ethoxyhydrophosphoryl)phenyl)(phenyl)methyl)carbamate

: 107-08-4
1-iodo-propane

: 1428526-86-6
tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate

Guidance literature:: tert-butyl N-((4-(ethoxyhydrophosphoryl)phenyl)(phenyl)methyl)carbamate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

1-iodo-propane; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 90-90-4
(4-bromophenyl)(phenyl)methanone

: 1428526-86-6
tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 24 h / 185 °C

2.1: potassium hydroxide / methanol / 8 h / Reflux

3.1: triethylamine / dichloromethane / 0 °C

3.2: 20 °C

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; anilinium hypophosphite; triethylamine / tetrahydrofuran / Reflux; Inert atmosphere

5.1: toluene / Reflux

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

6.2: 2 h / 20 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; anilinium hypophosphite; triethylamine; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 55095-17-5,220441-81-6
(4-bromophenyl)(phenyl)methanamine

: 1428526-86-6
tert-butyl N-{[4-(ethoxy(propyl)phosphoryl)phenyl](phenyl)methyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0 °C

1.2: 20 °C

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; anilinium hypophosphite; triethylamine / tetrahydrofuran / Reflux; Inert atmosphere

3.1: toluene / Reflux

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; anilinium hypophosphite; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene;