(Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1283231-60-6
Molecular Formula:C₁₇H₂₅BO₃
Molecular Weight:288.195
Hs Code.:

Synonyms:(Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of (Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 2 articles about (Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 73183-34-3
bis(pinacol)diborane

: 197250-99-0
1-(but-1-yn-1-yl)-4-methoxybenzene

: 1283231-60-6
(Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: bis(pinacol)diborane; With potassium tert-butylate; tris-(o-tolyl)phosphine; copper(l) chloride; In tetrahydrofuran; for 0.166667h; Inert atmosphere;

1-(but-1-yn-1-yl)-4-methoxybenzene; With methanol; In tetrahydrofuran; at 50 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1039/c0cc04496b

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: 197250-99-0
1-(but-1-yn-1-yl)-4-methoxybenzene

: 1283231-60-6
(Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: CH₃OC₆H₄C(CHCH₂CH₃)B(O₂C₂(CH₃)4)

Guidance literature:: With catalyst: CuCl/P(p-C₆H₄CH₃)3; methanol; sodium tert-butylate; In tetrahydrofuran; 1.1 equiv. of B compd., 2 equiv. of methanol, at 50°C for 24 h;
DOI:10.1039/c0cc04496b

Reference yield: 92.0%

: 591-50-4
iodobenzene

: 1283231-60-6
(Z)-2-(1-(4-methoxyphenyl)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: C₁₇H₁₈O

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium hydroxide; In water; toluene; at 70 ℃; for 24h; diastereoselective reaction;
DOI:10.1039/c9sc06136c