Technology Process of C19H19ClO2
There total 8 articles about C19H19ClO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
water; acetone;
at 120 ℃;
for 0.166667h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium hydroxide / ethanol / 20 h / Reflux
2.1: dihydrogen peroxide; selenium(IV) oxide / water; tert-butyl alcohol / 96 h / 20 °C
3.1: sodium methylate / methanol; N,N-dimethyl-formamide / 1.92 h / 80 °C
4.1: potassium carbonate / acetone / 18 h / 20 °C
5.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tert-butyl methyl ether / 0.25 h / Inert atmosphere
5.2: 1 h / 80 °C / Inert atmosphere; Microwave irradiation
6.1: potassium carbonate; palladium dichloride / methanol; water; toluene / 2 h / 80 °C
7.1: hydrogenchloride / water; acetone / 0.17 h / 120 °C / Microwave irradiation
With
hydrogenchloride; selenium(IV) oxide; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; dihydrogen peroxide; sodium methylate; potassium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; potassium hydroxide; palladium dichloride;
In
methanol; ethanol; tert-butyl methyl ether; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dihydrogen peroxide; selenium(IV) oxide / water; tert-butyl alcohol / 96 h / 20 °C
2.1: sodium methylate / methanol; N,N-dimethyl-formamide / 1.92 h / 80 °C
3.1: potassium carbonate / acetone / 18 h / 20 °C
4.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tert-butyl methyl ether / 0.25 h / Inert atmosphere
4.2: 1 h / 80 °C / Inert atmosphere; Microwave irradiation
5.1: potassium carbonate; palladium dichloride / methanol; water; toluene / 2 h / 80 °C
6.1: hydrogenchloride / water; acetone / 0.17 h / 120 °C / Microwave irradiation
With
hydrogenchloride; selenium(IV) oxide; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; dihydrogen peroxide; sodium methylate; potassium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; palladium dichloride;
In
methanol; tert-butyl methyl ether; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;