3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one

Base Information

Chemical Name:3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one
CAS No.:1615211-71-6
Molecular Formula:C₂₀H₂₁ClO₂
Molecular Weight:328.839
Hs Code.:

Synonyms:3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one

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Chemical Property of 3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one

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Technology Process of 3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one

There total 7 articles about 3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624-66-8
1-iodo-1-propyne

: 1615211-70-5
3-[2-chloro-6-ethyl-4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]-4-methoxybicyclo[3.2.1]oct-3-en-2-one

: 1615211-71-6
3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one

Guidance literature:: With potassium carbonate; palladium dichloride; In methanol; water; toluene; at 80 ℃; for 2h;

Reference yield:

: 1615211-66-9
3-[1-(2-chloro-6-ethylphenyl)methylidene]bicyclo[2.2.1]heptan-2-one

: 1615211-71-6
3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: dihydrogen peroxide; selenium(IV) oxide / water; tert-butyl alcohol / 96 h / 20 °C

2.1: sodium methylate / methanol; N,N-dimethyl-formamide / 1.92 h / 80 °C

3.1: potassium carbonate / acetone / 18 h / 20 °C

4.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tert-butyl methyl ether / 0.25 h / Inert atmosphere

4.2: 1 h / 80 °C / Inert atmosphere; Microwave irradiation

5.1: potassium carbonate; palladium dichloride / methanol; water; toluene / 2 h / 80 °C

With selenium(IV) oxide; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; dihydrogen peroxide; sodium methylate; potassium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; palladium dichloride; In methanol; tert-butyl methyl ether; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 3-(2-chloro-6-ethylphenyl)bicyclo[3.2.1]octane-2,4-dione

: 1615211-71-6
3-(2-chloro-6-ethyl-4-prop-1-ynylphenyl)-4-methoxybicyclo[3.2.1 ]oct-3-en-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 18 h / 20 °C

2.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tert-butyl methyl ether / 0.25 h / Inert atmosphere

2.2: 1 h / 80 °C / Inert atmosphere; Microwave irradiation

3.1: potassium carbonate; palladium dichloride / methanol; water; toluene / 2 h / 80 °C

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; potassium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; palladium dichloride; In methanol; tert-butyl methyl ether; water; acetone; toluene;