C₂₆H₂₃N₇O₂S

Base Information

Chemical Name:C₂₆H₂₃N₇O₂S
CAS No.:1430822-09-5
Molecular Formula:C₂₆H₂₃N₇O₂S
Molecular Weight:497.58
Hs Code.:

C<sub>26</sub>H<sub>23</sub>N<sub>7</sub>O<sub>2</sub>S

Synonyms:C₂₆H₂₃N₇O₂S

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Chemical Property of C₂₆H₂₃N₇O₂S

Chemical Property:

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Technology Process of C₂₆H₂₃N₇O₂S

There total 5 articles about C₂₆H₂₃N₇O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 51-45-6
histamine

: 1430822-07-3
C₂₁H₁₆N₄O₃S

: 1430822-09-5
C₂₆H₂₃N₇O₂S

Guidance literature:: C₂₁H₁₆N₄O₃S; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; at 0 - 20 ℃; for 2h; Inert atmosphere;

histamine; In 1,4-dioxane; at 50 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.ejmech.2013.01.019

Reference yield:

: 34761-09-6
ethyl 3-aminobenzothiophene-2-carboxylate

: 1430822-09-5
C₂₆H₂₃N₇O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium nitrite; acetic acid / water / 0.5 h / -5 °C

1.2: 3 h / 20 °C

2.1: sodium ethanolate / ethanol / 0.25 h / 20 °C

2.2: 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

4.1: potassium hydroxide / ethanol; water / 20 °C

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane / 2 h / 0 - 20 °C / Inert atmosphere

5.2: 12 h / 50 °C / Inert atmosphere

With dmap; sodium ethanolate; potassium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium nitrite; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.01.019

Reference yield:

: 1430822-01-7
3-phenylbenzo[4,5]thieno[2,3-e][1,2,3]triazolo[1,5-a]pyrimidin-5(4H)-one

: 1430822-09-5
C₂₆H₂₃N₇O₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

2.1: potassium hydroxide / ethanol; water / 20 °C

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 12 h / 50 °C / Inert atmosphere

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.01.019