8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Base Information

Chemical Name:8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene
CAS No.:72874-30-7
Molecular Formula:C₁₉H₁₆Cl₂N₄
Molecular Weight:371.269
Hs Code.:

Synonyms:8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

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Technology Process of 8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

There total 2 articles about 8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Chloro-butyric acid N'-(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl)-hydrazide

: 72874-30-7
8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: In acetic acid; for 0.333333h; Yield given; Heating;
DOI:10.1021/jm00178a009

Reference yield:

: 18091-89-9,112393-62-1
7-chloro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine

: 72874-30-7
8-Chloro-1-(3-chloro-propyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1.58 h / 0 - 20 °C

2: acetic acid / 0.33 h / Heating

In tetrahydrofuran; acetic acid;
DOI:10.1021/jm00178a009