methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

Base Information

Chemical Name:methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate
CAS No.:1379603-28-7
Molecular Formula:C₅₅H₅₆N₄O₁₀
Molecular Weight:933.07
Hs Code.:

methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

Synonyms:methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

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Chemical Property of methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

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Technology Process of methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

There total 5 articles about methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1379586-98-7
methyl (S)-2-(3-((benzyloxy)carbonyl)thioureido)propanoate

: 1379587-21-9
benzyl (S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-((bis(4-methoxyphenyl)methyl)amino)pentanoate

: 1379603-28-7
methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

Guidance literature:: With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja301994d

Reference yield:

: 7525-23-7
4,4'-dimethoxydiphenylmethyl chloride

: 1379603-28-7
methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; mercury dichloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With triethylamine; mercury dichloride; In dichloromethane;
DOI:10.1021/ja301994d

Reference yield:

: 1379586-97-6
benzyl (S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-aminopentanoate hydrochloride

: 1379603-28-7
methyl (5S,12S,Z)-5-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)imino)-9-(bis(4-methoxyphenyl)methyl)-1-(9H-fluoren-9-yl)-12-methyl-3-oxo-2-oxa-4,9,11-triazatridecan-13-oate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; mercury dichloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With triethylamine; mercury dichloride; In dichloromethane;
DOI:10.1021/ja301994d