4-methyl-3,5-dibenzyloxybenzoic acid

Base Information Edit

Chemical Name:4-methyl-3,5-dibenzyloxybenzoic acid
CAS No.:34696-32-7
Molecular Formula:C₂₂H₂₀O₄
Molecular Weight:348.398
Hs Code.:
Mol file:34696-32-7.mol

Synonyms:4-methyl-3,5-dibenzyloxybenzoic acid

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Chemical Property of 4-methyl-3,5-dibenzyloxybenzoic acid Edit

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Technology Process of 4-methyl-3,5-dibenzyloxybenzoic acid

There total 4 articles about 4-methyl-3,5-dibenzyloxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 28026-96-2
3,5-dihydroxy-4-methylbenzoic acid

: 100-39-0
benzyl bromide

: 34696-32-7
4-methyl-3,5-dibenzyloxybenzoic acid

Guidance literature:: 3,5-dihydroxy-4-methylbenzoic acid; benzyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; for 12h;

With potassium hydroxide; In methanol; for 1h; Reflux;

With hydrogenchloride; In methanol; water; pH=2 - 3;

Reference yield:

: 34696-31-6
methyl 3,5-bis(benzyloxy)-4-methylbenzoate

: 34696-32-7
4-methyl-3,5-dibenzyloxybenzoic acid

Guidance literature:: With sodium hydroxide; In ethanol;
DOI:10.1039/j39710003566

Reference yield:

: 3899-19-2
2,5-dihydroxy-4-methylbenzoic acid methyl ester

: 34696-32-7
4-methyl-3,5-dibenzyloxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone

2: aq. NaOH / ethanol

With sodium hydroxide; potassium carbonate; In ethanol; acetone;
DOI:10.1039/j39710003566