CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)^(1-)*HN(CH(CH₃)2)2C₂H₅⁽¹⁺⁾=HN(CH(CH₃)2)2C₂H₅CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)

Base Information

• Chemical Name: CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)^(1-)*HN(CH(CH₃)2)2C₂H₅⁽¹⁺⁾=HN(CH(CH₃)2)2C₂H₅CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)
• CAS No.: 875765-21-2
• Molecular Formula: C₈H₂₀N*C₂₁H₂₁ClO₅PPdS
• Molecular Weight: 688.561
• Mol file: 875765-21-2.mol

Synonyms:CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)^(1-)*HN(CH(CH₃)2)2C₂H₅⁽¹⁺⁾=HN(CH(CH₃)2)2C₂H₅CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)

Chemical Property of CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)^(1-)*HN(CH(CH₃)2)2C₂H₅⁽¹⁺⁾=HN(CH(CH₃)2)2C₂H₅CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)^(1-)*HN(CH(CH₃)2)2C₂H₅⁽¹⁺⁾=HN(CH(CH₃)2)2C₂H₅CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)

There total 2 articles about CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)^(1-)*HN(CH(CH₃)2)2C₂H₅⁽¹⁺⁾=HN(CH(CH₃)2)2C₂H₅CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

chloromethyl(1,5-cyclooctadiene)palladium(II) + N-ethyl-N,N-diisopropylamine (7087-68-5) + 2-{bis(2-methoxyphenyl)phosphino}benzenesulphonic acid (257290-43-0) → NHCH2CH3(CH(CH3)2)2(1+)*PdCH3Cl((CH3OC6H4)2PC6H4SO3)(1-)=NHCH2CH3(CH(CH3)2)2PdCH3Cl((CH3OC6H4)2PC6H4SO3) (875765-21-2)

Guidance literature:

In dichloromethane; react. of amine with ligand in CH2Cl2 at room temp. for 10 min, addn. ofpalladium complex, react. at room temp. for 1 h;

DOI:10.1039/b512452m

Reference yield:

chloromethyl(1,5-cyclooctadiene)palladium(II) + N-ethyl-N,N-diisopropylamine (7087-68-5) + 2-{bis(2-methoxyphenyl)phosphino}benzenesulphonic acid (257290-43-0) → CH3PdCl(O3SC6H4P(C6H4OCH3)2)(1-)*HN(CH(CH3)2)2C2H5(1+)=HN(CH(CH3)2)2C2H5CH3PdCl(O3SC6H4P(C6H4OCH3)2) (875765-21-2)

Guidance literature:

In dichloromethane; treatment of phospine ligand with (i-Pr)2NEt for 10 min at room temp. inCH2Cl2 ,treatment with PdMeCl(C8H12) for 1 h at room temp.;

DOI:10.1021/ja0725504

Reference yield: 68.0%

2,6-dimethylpyridine (108-48-5) + CH3PdCl(O3SC6H4P(C6H4OCH3)2)(1-)*HN(CH(CH3)2)2C2H5(1+)=HN(CH(CH3)2)2C2H5CH3PdCl(O3SC6H4P(C6H4OCH3)2) (875765-21-2) → [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)] (925941-62-4)

Guidance literature:

With potassium carbonate; In dichloromethane; treatment of Pd complex with 2,6-lutidine and K2CO3 for 1 h at room temp. in CH2Cl2;

DOI:10.1021/ja0725504

upstream raw materials:

N-ethyl-N,N-diisopropylamine

2-{bis(2-methoxyphenyl)phosphino}benzenesulphonic acid

Downstream raw materials:

[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]