[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid

Base Information

Chemical Name:[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid
CAS No.:210036-01-4
Molecular Formula:C₂₁H₁₉N₅O₇
Molecular Weight:453.411
Hs Code.:

Synonyms:[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid

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Chemical Property of [(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid

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Technology Process of [(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid

There total 2 articles about [(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 124676-23-9
α-(N-benzyloxycarbonyl)aminoglycine

: 204527-99-1
1-Benzyl-5-nitro-1H-imidazole-4-carboxylic acid pentafluorophenyl ester

: 210036-01-4
[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 2h;
DOI:10.1080/07328319808004227

Reference yield:

: 69195-96-6
5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid

: 210036-01-4
[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-benzyloxycarbonylamino-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / DCC, EtOAc / dimethylformamide / 3 h / 0 - 20 °C

2: 85 percent / Et₃N / CHCl₃ / 11 h / Ambient temperature

With ethyl acetate; triethylamine; dicyclohexyl-carbodiimide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(98)00672-6