Technology Process of C26H42O7S2Si
There total 11 articles about C26H42O7S2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
carbon disulfide; C24H40O7Si;
With
sodium hydride;
In
tetrahydrofuran;
at 0 ℃;
methyl iodide;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2012.06.005
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: boron trifluoride diethyl etherate / diethyl ether / 0 °C
2.1: sodium periodate; ruthenium trichloride; water; zinc(II) chloride / ethyl acetate; acetonitrile / 0 °C
3.1: toluene-4-sulfonic acid / tetrahydrofuran / 40 °C
4.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C
5.1: sodium hydride / tetrahydrofuran / 0 °C
5.2: 0 - 20 °C
With
ruthenium trichloride; sodium tetrahydroborate; sodium periodate; boron trifluoride diethyl etherate; water; sodium hydride; toluene-4-sulfonic acid; zinc(II) chloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2012.06.005
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium periodate; ruthenium trichloride; water; zinc(II) chloride / ethyl acetate; acetonitrile / 0 °C
2.1: toluene-4-sulfonic acid / tetrahydrofuran / 40 °C
3.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C
4.1: sodium hydride / tetrahydrofuran / 0 °C
4.2: 0 - 20 °C
With
ruthenium trichloride; sodium tetrahydroborate; sodium periodate; water; sodium hydride; toluene-4-sulfonic acid; zinc(II) chloride;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2012.06.005
