1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

Base Information

Chemical Name:1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate
CAS No.:1160707-41-4
Molecular Formula:C₃₁H₃₈IN₅O₁₀S
Molecular Weight:799.641
Hs Code.:

1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

Synonyms:1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

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Chemical Property of 1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

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Technology Process of 1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

There total 5 articles about 1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1160707-38-9
C₂₈H₂₅IN₆O₈

: 367-93-1
isopropyl β-D-thiogalactopyranoside

: 1160707-41-4
1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

Guidance literature:: With pyridine; dmap;

Reference yield:

: 1160707-35-6
1-[2-hydroxy-2-(4-hydroxyphenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

: 1160707-41-4
1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 20 °C

2.1: N-chloro-succinimide; chloro-trimethyl-silane / dichloromethane / 1.5 h

2.2: 1.5 h / 20 °C

3.1: triethylamine / dichloromethane / 4 h

4.1: dmap; pyridine

With pyridine; dmap; N-chloro-succinimide; chloro-trimethyl-silane; potassium tert-butylate; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc37826d

Reference yield:

: 1198-84-1
4-hydroxymandelic acid

: 1160707-41-4
1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl (3,4,5-trihydroxy-6-(isopropylthio)tetrahydro-2H-pyran-2-yl)methylcarbonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / N,N-dimethyl-formamide

2.1: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 20 °C

3.1: N-chloro-succinimide; chloro-trimethyl-silane / dichloromethane / 1.5 h

3.2: 1.5 h / 20 °C

4.1: triethylamine / dichloromethane / 4 h

5.1: dmap; pyridine

With pyridine; dmap; N-chloro-succinimide; chloro-trimethyl-silane; potassium tert-butylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc37826d