5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide

Base Information

Chemical Name:5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide
CAS No.:1451273-65-6
Molecular Formula:C₁₉H₁₄ClF₃N₂O₄S
Molecular Weight:458.845
Hs Code.:

Synonyms:5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide

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Chemical Property of 5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide

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Technology Process of 5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide

There total 4 articles about 5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 77797-64-9
5-chloro-2-(trifluoromethoxy)benzene-1-sulfonyl chloride

: 1225522-97-3
5-(4-methoxyphenyl)pyridin-3-amine

: 1451273-65-6
5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide

Guidance literature:: With dmap; In pyridine; at 70 ℃; for 4h;

Reference yield:

: 13535-01-8
3-amino-5-bromopyridine

: 1451273-65-6
5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / N,N-dimethyl-formamide; water / 0.17 h / 120 °C / Inert atmosphere; Microwave irradiation

2: dmap / pyridine / 4 h / 70 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In pyridine; water; N,N-dimethyl-formamide;

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1451273-65-6
5-chloro-N-[5-(4-methoxyphenyl)pyridin-3-yl]-2-trifluoromethoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / N,N-dimethyl-formamide; water / 0.17 h / 120 °C / Inert atmosphere; Microwave irradiation

2: dmap / pyridine / 4 h / 70 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In pyridine; water; N,N-dimethyl-formamide;