4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

Base Information

Chemical Name:4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid
CAS No.:186256-53-1
Molecular Formula:C₅₆H₅₈OS
Molecular Weight:779.142
Hs Code.:

Synonyms:4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

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Chemical Property of 4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

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Technology Process of 4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

There total 3 articles about 4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: C₆₀H₆₆OS

: 186256-53-1
4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

Guidance literature:: at 225 ℃;
DOI:10.1021/ja962994s

Reference yield: 41.0%

: 177971-45-8
4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

: 186256-53-1
4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

Guidance literature:: With iodosylbenzene; In chloroform; Ambient temperature;
DOI:10.1021/ja962994s

Reference yield:

: 1-[4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyldisulfanyl]-4-mercapto-butane-2,3-diol

: 186256-53-1
4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

Guidance literature:: Multi-step reaction with 2 steps

1: SiO₂

2: 41 percent / PhIO / CHCl₃ / Ambient temperature

With iodosylbenzene; silica gel; In chloroform;
DOI:10.1021/ja962994s