S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

Base Information

Chemical Name:S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol
CAS No.:406675-51-2
Molecular Formula:C₅₆H₅₇NOS
Molecular Weight:792.141
Hs Code.:

Synonyms:S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

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Chemical Property of S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

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Technology Process of S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

There total 4 articles about S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 406675-53-4
C₅₆H₅₇NO₂S

: 406675-51-2
S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

Guidance literature:: With triphenylphosphine; In chloroform; for 0.0833333h;

Reference yield: 85.0%

: 177971-45-8
4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

: 406675-51-2
S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

Guidance literature:: With tert.-butylnitrite; In chloroform; at 20 ℃; for 0.333333h;

Reference yield:

: 186256-53-1
4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)methyl]benzenesulfenic acid

: 406675-51-2
S-nitroso-4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / CH₂Cl₂ / 20 °C

2: SiO₂

3: 85 percent / t-BuONO / CH₂Cl₂ / 20 °C

With tert.-butylnitrite; silica gel; In dichloromethane;
DOI:10.1002/hc.10068