1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole

Base Information

Chemical Name:1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole
CAS No.:1056263-24-1
Molecular Formula:C₂₇H₂₁FN₂O₂
Molecular Weight:424.474
Hs Code.:

Synonyms:1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole

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Chemical Property of 1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole

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Technology Process of 1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole

There total 2 articles about 1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81382-45-8
4-hydroxyindazole

: 1056263-24-1
1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 2 h / 20 °C

2.1: triethylamine / copper diacetate / dichloromethane / 64 h / 20 °C / Molecular sieve

With sodium hydride; triethylamine; copper diacetate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 1056263-24-1
1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 2 h / 20 °C

2.1: triethylamine / copper diacetate / dichloromethane / 64 h / 20 °C / Molecular sieve

With sodium hydride; triethylamine; copper diacetate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1056263-24-1
1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-[(phenylmethyl)oxy]-1H-indazole

: 1056261-59-6
1-(3-fluoro-4-hydroxyphenyl)-1H-indazol-4-ol

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; ethyl acetate; at 20 ℃; for 3h; under 760.051 Torr; Product distribution / selectivity;