C₁₇H₂₃NO₆S

Base Information

• Chemical Name: C₁₇H₂₃NO₆S
• CAS No.: 1309587-71-0
• Molecular Formula: C₁₇H₂₃NO₆S
• Molecular Weight: 369.439
• Mol file: 1309587-71-0.mol

Synonyms:C₁₇H₂₃NO₆S

Chemical Property of C₁₇H₂₃NO₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₃NO₆S

There total 7 articles about C₁₇H₂₃NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H13NO3 → C17H23NO6S (1309587-71-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -50 °C / Inert atmosphere

1.2: 1.17 h / -50 °C / Inert atmosphere

2.1: potassium carbonate / 12 h / 23 °C / Inert atmosphere

With n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane;

DOI:10.1021/ja203227q

Reference yield:

C16H19NO3 → C17H23NO6S (1309587-71-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ammonia; sodium; tert-butyl alcohol / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -50 °C / Inert atmosphere

2.2: 1.17 h / -50 °C / Inert atmosphere

3.1: potassium carbonate / 12 h / 23 °C / Inert atmosphere

With n-butyllithium; ammonia; sodium; potassium carbonate; tert-butyl alcohol; In tetrahydrofuran; hexane;

DOI:10.1021/ja203227q

Reference yield:

C23H19NO5 → C17H23NO6S (1309587-71-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: quinoline; copper(I) oxide; water / 0.42 h / 150 °C / Inert atmosphere; Microwave irradiation

2.1: toluene-4-sulfonic acid / methanol / 14 h / Reflux; Inert atmosphere

3.1: ammonia; sodium; tert-butyl alcohol / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -50 °C / Inert atmosphere

4.2: 1.17 h / -50 °C / Inert atmosphere

5.1: potassium carbonate / 12 h / 23 °C / Inert atmosphere

With quinoline; copper(I) oxide; n-butyllithium; ammonia; water; sodium; potassium carbonate; toluene-4-sulfonic acid; tert-butyl alcohol; In tetrahydrofuran; methanol; hexane;

DOI:10.1021/ja203227q

upstream raw materials:

methanol

5-benzyloxy-N-benzylpyridine-2-one

p-toluenesulfonyl chloride