[5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide

Base Information

Chemical Name:[5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide
CAS No.:887703-80-2
Molecular Formula:Br*C₃₉H₃₆FN₃OP
Molecular Weight:692.611
Hs Code.:

Synonyms:[5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide

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Technology Process of [5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide

There total 1 articles about [5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 887703-79-9
1-(4-fluorophenyl)-5-hydroxymethyl-4-isopropyl-1H-pyrazole-3-carboxylic acid benzylamide

: 6399-81-1
triphenylphosphine hydrobromide

: 887703-80-2
[5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide

Guidance literature:: In acetonitrile; at 80 ℃; for 24h;

Reference yield:

: 887703-80-2
[5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide

: 124752-23-4
tert-butyl 2-[(4R,6S)-6-formyl-2,2-dimethyl-1,3-dioxan-4-yl]acetate

: 887703-81-3
(6-{2-[5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-yl]vinyl}-2,2-dimethyl-[1R,3R]dioxan-4-yl)acetic acid tert-butyl ester

Guidance literature:: [5-benzylcarbamoyl-2-(4-fluorophenyl)-4-isopropyl-2H-pyrazol-3-ylmethyl]triphenylphosphonium bromide; With lithium hexamethyldisilazane; In tetrahydrofuran; dimethyl sulfoxide; at -78 ℃; for 0.0833333h;

tert-butyl 2-[(4R,6S)-6-formyl-2,2-dimethyl-1,3-dioxan-4-yl]acetate; In tetrahydrofuran; dimethyl sulfoxide; at -78 - 25 ℃; Further stages.;
DOI:10.1021/jm070849r