N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid

Base Information

Chemical Name:N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid
CAS No.:1227868-03-2
Molecular Formula:C₃₃H₃₀N₂O₂Si
Molecular Weight:514.699
Hs Code.:

Synonyms:N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid

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Chemical Property of N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid

Chemical Property:

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Technology Process of N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid

There total 5 articles about N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(4-(trimethylsilyl)phenyl)-N-phenyl-4-(4-aminostyryl)benzaldehyde

: 372-09-8
cyanoacetic acid

: 1227868-03-2
N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid

Guidance literature:: With piperidine; In acetonitrile; for 12h; Reflux;

Reference yield:

: 62-53-3
aniline

: 1227868-03-2
N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 24 h / 100 °C

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate / toluene / 24 h / 100 °C

3: sodium t-butanolate / tetrahydrofuran / 12 h / 20 °C

4: sodium t-butanolate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) / N,N-dimethyl acetamide / 24 h / 80 °C

5: piperidine / acetonitrile / 12 h / Reflux

With piperidine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); tri-tert-butyl phosphine; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In tetrahydrofuran; N,N-dimethyl acetamide; toluene; acetonitrile;

Reference yield:

: 13024-18-5
4-(trimethylsilyl)-N-phenylbenzeneamine

: 1227868-03-2
N-((4-trimethylsilyl)phenyl)-N-phenyl-4-((4-aminostyryl)-2-cyano)-3-phenylacrylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate / toluene / 24 h / 100 °C

2: sodium t-butanolate / tetrahydrofuran / 12 h / 20 °C

3: sodium t-butanolate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) / N,N-dimethyl acetamide / 24 h / 80 °C

4: piperidine / acetonitrile / 12 h / Reflux

With piperidine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); tri-tert-butyl phosphine; sodium t-butanolate; In tetrahydrofuran; N,N-dimethyl acetamide; toluene; acetonitrile;