1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime

Base Information

• Chemical Name: 1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime
• CAS No.: 1574525-81-7
• Molecular Formula: C₁₄H₂₂N₂O₄
• Molecular Weight: 282.34
• Mol file: 1574525-81-7.mol

Synonyms:1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime

Chemical Property of 1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime

There total 1 articles about 1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(1-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone (1574525-82-8) → 1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime (1574525-81-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 4h; Reflux; Inert atmosphere;

DOI:10.1002/chem.201304740

Reference yield:

manganese(II) bromide tetrahydrate + benzene-1,3,5-tricarboxylic acid (554-95-0) + 1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime (1574525-81-7) → [MnIII12O4((1-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime)8((1-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime)4(trimesate)4] hydrate

Guidance literature:

With triethylamine; In methanol; for 3h;

DOI:10.1039/c4dt01469c

Reference yield:

methanol (67-56-1) + manganese(II) chloride tetrahydrate + 1-((3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone oxime (1574525-81-7) → 4C14H18N2O4(4-)*20CH3O(1-)*12Mn(3+)

Guidance literature:

With triethylamine; sodium t-butanolate; for 3h;

DOI:10.1039/c3cc49583c

upstream raw materials:

(1-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methyl)phenyl)ethanone