rac-N-glycine ethyl ester

Base Information

Chemical Name:rac-N-glycine ethyl ester
CAS No.:112681-25-1
Molecular Formula:C₁₂H₁₅NO₄
Molecular Weight:237.255
Hs Code.:

rac-N-<hydroxy(phenyl)acetyl>glycine ethyl ester

Synonyms:rac-N-glycine ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-N-glycine ethyl ester

Chemical Property:

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Technology Process of rac-N-glycine ethyl ester

There total 4 articles about rac-N-glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 2999-46-4
Ethyl isocyanoacetate

: 100-52-7
benzaldehyde

: 112681-25-1
rac-N-glycine ethyl ester

Guidance literature:: Ethyl isocyanoacetate; benzaldehyde; With pyridine N-oxide; tetrachlorosilane; In dichloromethane; at -74 ℃; for 24h;

With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ja035410c

Reference yield:

: [1-Chloro-2-phenyl-2-trichlorosilanyloxy-eth-(Z)-ylideneamino]-acetic acid ethyl ester

: 112681-25-1
rac-N-glycine ethyl ester

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 2h;
DOI:10.1021/jo050549m

Reference yield:

: 100-52-7
benzaldehyde

: 112681-25-1
rac-N-glycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine N-oxide; SiCl₄ / CH₂Cl₂ / 4 h / -74 °C

2: 104 mg / NaHCO₃ / H₂O; CH₂Cl₂ / 2 h / 20 °C

With pyridine N-oxide; tetrachlorosilane; sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1021/jo050549m