C₂₂H₁₅F₃N₂O₃S

Base Information

Chemical Name:C₂₂H₁₅F₃N₂O₃S
CAS No.:950857-59-7
Molecular Formula:C₂₂H₁₅F₃N₂O₃S
Molecular Weight:444.434
Hs Code.:

C<sub>22</sub>H<sub>15</sub>F<sub>3</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:C₂₂H₁₅F₃N₂O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₅F₃N₂O₃S

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Technology Process of C₂₂H₁₅F₃N₂O₃S

There total 4 articles about C₂₂H₁₅F₃N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 950857-44-0
C₁₅H₁₂F₃NO₃S

: 3058-39-7
4-iodobenzonitrile

: 950857-59-7
C₂₂H₁₅F₃N₂O₃S

Guidance literature:: With potassium carbonate; copper(l) iodide; In 1,2-dimethoxyethane; at 80 ℃; for 3h;

Reference yield:

: 950857-36-0
5-iodo-6-methyl-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxylic acid

: 950857-59-7
C₂₂H₁₅F₃N₂O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: methanol; hexane; toluene

2: copper(l) iodide; potassium carbonate / 1,2-dimethoxyethane / 17 h / 90 °C

3: trifluoroacetic acid / dichloroethane, 1,1- / 17 h / Heating / reflux

4: copper(l) iodide; potassium carbonate / 1,2-dimethoxyethane / 3 h / 80 °C

With copper(l) iodide; potassium carbonate; trifluoroacetic acid; In methanol; 1,2-dimethoxyethane; dichloroethane, 1,1-; hexane; toluene;

Reference yield:

: 694479-56-6
6-methyl-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxylic acid

: 950857-59-7
C₂₂H₁₅F₃N₂O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: N-iodo-succinimide / dichloromethane; trifluoroacetic acid / 1.5 h

2: methanol; hexane; toluene

3: copper(l) iodide; potassium carbonate / 1,2-dimethoxyethane / 17 h / 90 °C

4: trifluoroacetic acid / dichloroethane, 1,1- / 17 h / Heating / reflux

5: copper(l) iodide; potassium carbonate / 1,2-dimethoxyethane / 3 h / 80 °C

With N-iodo-succinimide; copper(l) iodide; potassium carbonate; trifluoroacetic acid; In methanol; 1,2-dimethoxyethane; dichloroethane, 1,1-; hexane; dichloromethane; toluene; trifluoroacetic acid;