5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole
CAS No.:1333237-40-3
Molecular Formula:C₂₃H₃₀Cl₄N₄O₆S
Molecular Weight:632.392
Hs Code.:

Synonyms:5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole

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Chemical Property of 5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole

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Technology Process of 5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole

There total 14 articles about 5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: C₁₇H₂₂Cl₄N₄O₆S

: 67-64-1
acetone

: 1333237-40-3
5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With toluene-4-sulfonic acid; copper(II) sulfate; for 20h; Inert atmosphere;
DOI:10.1002/anie.201102521

Reference yield: 82.0%

: 1333237-39-0
5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)thio)-1-phenyl-1H-tetrazole

: 1333237-40-3
5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With ammonium molybdate tetrahydrate; dihydrogen peroxide; In tetrahydrofuran; ethanol; water; at 60 ℃; for 3h;
DOI:10.1021/jacs.9b05013

Reference yield: 61.0%

: 1333237-39-0
5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)thio)-1-phenyl-1H-tetrazole

: C₁₇H₂₂Cl₄N₄O₆S

: 1333237-40-3
5-((((4S,5S,6R)-5-chloro-2,2-dimethyl-6-((S)-1,1,4-trichloro-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)butyl)-1,3-dioxan-4-yl)methyl)sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 40 ℃; for 22h; Inert atmosphere;
DOI:10.1002/anie.201102521