(S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

Base Information

Chemical Name:(S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide
CAS No.:107994-49-0
Molecular Formula:C₂₉H₃₆N₄O₄S*HI
Molecular Weight:664.608
Hs Code.:

(S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

Synonyms:(S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

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Chemical Property of (S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

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Technology Process of (S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

There total 8 articles about (S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 107994-45-6
(S)-2-[2-Oxo-2-piperidin-1-yl-1-(4-thiocarbamoyl-benzyl)-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester

: 74-88-4
methyl iodide

: 107994-49-0
(S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

Guidance literature:: In acetone; for 0.25h; Heating;

Reference yield:

: 110-89-4
piperidine

: 107994-49-0
(S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: ethyl acetate / 1 h / Ambient temperature

2: 55 percent / H₂S / pyridine; triethylamine / 72 h / Ambient temperature

3: 70 percent / acetone / 0.25 h / Heating

With hydrogen sulfide; In pyridine; ethyl acetate; triethylamine; acetone;

Reference yield:

: 105414-01-5,102988-94-3
Cbz-L-Pro-OCO₂-i-Bu

: 107994-49-0
(S)-2-[1-(4-Methylsulfanylcarbonimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethylcarbamoyl]-pyrrolidine-1-carboxylic acid benzyl ester; hydriodide

Guidance literature:: Multi-step reaction with 5 steps

1: TEA / ethyl acetate / 1 h, 0 deg C; 1 h, room temp.

2: 4-ethylmorpholine / ethyl acetate / 0.25 h / 0 °C

3: ethyl acetate / 1 h / Ambient temperature

4: 55 percent / H₂S / pyridine; triethylamine / 72 h / Ambient temperature

5: 70 percent / acetone / 0.25 h / Heating

With N-ethylmorpholine;; TEA; hydrogen sulfide; In pyridine; ethyl acetate; triethylamine; acetone;