[ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

Base Information

Chemical Name:[ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]
CAS No.:98481-42-6
Molecular Formula:C₃₉H₃₇ClNO₇P₂Re
Molecular Weight:915.333
Hs Code.:

[ReH(C<sub>2</sub>H<sub>5</sub>OHOClO<sub>3</sub>)(CO)(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)2]

Synonyms:[ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

Suppliers and Price of [ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

Chemical Property:

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Technology Process of [ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

There total 1 articles about [ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 98481-36-8
[ReH(OC₂H₅)(CO)(NO)(P(C₆H₅)3)2]

: 98481-42-6
[ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

Guidance literature:: With HClO₄; In diethyl ether; dichloromethane; addn. of 70% aq. HClO4 to a suspension of Re-complex in CH2Cl2 under N2; addn. of diethyl ether and stirring of the soln.;; pptn.; elem. anal.;;

Reference yield: 85.0%

: 98481-42-6
[ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

: 98481-47-1
[ReCl(OC₂H₅)(CO)(NO)(P(C₆H₅)3)2]*0.5CH₂Cl₂

Guidance literature:: With LiCl; CH₂Cl₂; In ethanol; dichloromethane; dissolving freshly prepared monohydride and LiCl in CH2Cl2-ethanol (1:1) under N2; stirring for 1 h; evapn. of CH2Cl2 in vacuum;; pptn.; elem. anal.;;

Reference yield: 78.0%

: 98481-42-6
[ReH(C₂H₅OHOClO₃)(CO)(NO)(P(C₆H₅)3)2]

: 10377-51-2
lithium iodide

: 98481-49-3
[ReI(OC₂H₅)(CO)(NO)(P(C₆H₅)3)2]

Guidance literature:: In ethanol; dichloromethane; dissolving freshly prepared monohydride and LiI in CH2Cl2-ethanol (1:1)under N2; stirring for 1 h; evapn. of CH2Cl2 in vacuum;; pptn.;;