(2E,4E)-5-Phenyl-penta-2,4-dienoicacidethylester

Base Information

Chemical Name:(2E,4E)-5-Phenyl-penta-2,4-dienoicacidethylester
CAS No.:39806-16-1
Molecular Formula:C13H14 O2
Molecular Weight:202.253
Hs Code.:
DSSTox Substance ID:DTXSID90699422
Mol file:39806-16-1.mol

Synonyms:SCHEMBL3685507;DTXSID90699422;(2E,4E)-5-PHENYL-PENTA-2,4-DIENOICACIDETHYLESTER

Suppliers and Price of (2E,4E)-5-Phenyl-penta-2,4-dienoicacidethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(2E,4E)-5-PHENYL-PENTA-2,4-DIENOIC ACID ETHYL ESTER 95.00%
5MG
$ 498.27

Total 4 raw suppliers

Chemical Property of (2E,4E)-5-Phenyl-penta-2,4-dienoicacidethylester

Chemical Property:

Boiling Point:135-136 °C(Press: 3 Torr)
PSA：26.30000
Density:1.045±0.06 g/cm3(Predicted)
LogP:2.81910
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:202.099379685
Heavy Atom Count:15
Complexity:235

Purity/Quality:

99% ^*data from raw suppliers

(2E,4E)-5-PHENYL-PENTA-2,4-DIENOIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C=CC=CC1=CC=CC=C1

Technology Process of (2E,4E)-5-Phenyl-penta-2,4-dienoicacidethylester

There total 91 articles about (2E,4E)-5-Phenyl-penta-2,4-dienoicacidethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 14371-10-9
(E)-3-phenylpropenal

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 39806-16-1
ethyl (2E,4E)-5-phenyl-penta-2,4-dienoate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

(E)-3-phenylpropenal; In tetrahydrofuran; mineral oil; at 0 - 22 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jacs.8b10885

Reference yield: 97.0%

: 623-73-4
diazoacetic acid ethyl ester

: 104-55-2
3-phenyl-propenal

: 38447-06-2,38448-85-0,39806-16-1,136265-12-8,1552-95-0,106925-11-5
(2E)-ethyl 5-phenylpenta-2,4-dienoate

Guidance literature:: With tributylstibine; copper(l) iodide; In benzene; at 50 ℃; for 4h;
DOI:10.1016/S0040-4039(00)97988-7

Reference yield: 96.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 104-55-2
3-phenyl-propenal

: 38447-06-2,38448-85-0,39806-16-1,136265-12-8,1552-95-0,106925-11-5
(2E)-ethyl 5-phenylpenta-2,4-dienoate

: 621-82-9
Cinnamic acid

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; 3-phenyl-propenal; With potassium carbonate; for 6h; Neat (no solvent); high-speed ball milling;

With Oxone; for 12h; optical yield given as %de; diastereoselective reaction; Neat (no solvent); high-speed ball milling;
DOI:10.1039/c0gc00671h