2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Base Information

Chemical Name:2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate
CAS No.:1370602-26-8
Molecular Formula:C₃₄H₅₆N₈O₂
Molecular Weight:608.871
Hs Code.:

2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Synonyms:2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Suppliers and Price of 2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

There total 7 articles about 2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.6%

: 108-01-0
2-(N,N-dimethylamino)ethanol

: 865061-29-6
3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionic acid

: 1370602-26-8
2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Guidance literature:: 2-(N,N-dimethylamino)ethanol; 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionic acid; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 20h;

With sodium hydroxide; In 1,4-dioxane; water; pH=9;

Reference yield:

: 1370602-24-6
ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

: 1370602-26-8
2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / ethanol / 5.5 h / 20 °C / Cooling with ice

1.2: pH 9

2.1: trimethyl orthoformate / ethanol / 19 h / 20 °C

2.2: 2 h / 20 °C / Cooling with ice

3.1: sodium tris(acetoxy)borohydride; ethanol / ethanol / 72 h / 20 °C

3.2: 2 h / 20 °C / Cooling with ice

4.1: sodium hydroxide / water / 4 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane / 20 h / 20 °C

5.2: pH 9

With hydrogenchloride; ethanol; sodium tris(acetoxy)borohydride; sodium hydroxide; trimethyl orthoformate; In 1,4-dioxane; ethanol; water;

Reference yield:

: 927885-21-0
N-{4-[(benzylideneamino)methyl]benzyl}-N',N'-dipropylbutane-1,4-diamine

: 1370602-26-8
2-dimethylaminoethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Guidance literature:: Multi-step reaction with 6 steps

1.1: ytterbium trifluoromethanesulfonate / acetonitrile; toluene / 92 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride / ethanol / 5.5 h / 20 °C / Cooling with ice

2.2: pH 9

3.1: trimethyl orthoformate / ethanol / 19 h / 20 °C

3.2: 2 h / 20 °C / Cooling with ice

4.1: sodium tris(acetoxy)borohydride; ethanol / ethanol / 72 h / 20 °C

4.2: 2 h / 20 °C / Cooling with ice

5.1: sodium hydroxide / water / 4 h / 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 20 h / 20 °C

6.2: pH 9

With hydrogenchloride; ytterbium trifluoromethanesulfonate; ethanol; sodium tris(acetoxy)borohydride; sodium hydroxide; trimethyl orthoformate; In 1,4-dioxane; ethanol; water; toluene; acetonitrile;