ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

Base Information

Chemical Name:ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate
CAS No.:1370602-24-6
Molecular Formula:C₃₀H₄₅N₃O₂
Molecular Weight:479.706
Hs Code.:

Synonyms:ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

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Chemical Property of ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

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Technology Process of ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

There total 3 articles about ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.5%

: 927885-21-0
N-{4-[(benzylideneamino)methyl]benzyl}-N',N'-dipropylbutane-1,4-diamine

: 140-88-5,9003-32-1
ethyl acrylate

: 1370602-24-6
ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

Guidance literature:: With ytterbium trifluoromethanesulfonate; In toluene; acetonitrile; at 20 ℃; for 92h; Inert atmosphere;

Reference yield:

: 927885-19-6
N-(4-aminomethylbenzyl)-N',N'-dipropylbutane-1,4-diamine

: 1370602-24-6
ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

Guidance literature:: Multi-step reaction with 2 steps

1: trimethyl orthoformate / methanol / 25 h / Inert atmosphere

2: ytterbium trifluoromethanesulfonate / acetonitrile; toluene / 92 h / 20 °C / Inert atmosphere

With ytterbium trifluoromethanesulfonate; trimethyl orthoformate; In methanol; toluene; acetonitrile;

Reference yield:

: 100-52-7
benzaldehyde

: 1370602-24-6
ethyl 3-[{4-[(benzylideneamino)methyl]benzyl}-(4-dipropylaminobutyl)amino]propionate

Guidance literature:: Multi-step reaction with 2 steps

1: trimethyl orthoformate / methanol / 25 h / Inert atmosphere

2: ytterbium trifluoromethanesulfonate / acetonitrile; toluene / 92 h / 20 °C / Inert atmosphere

With ytterbium trifluoromethanesulfonate; trimethyl orthoformate; In methanol; toluene; acetonitrile;