(2E)-azepan-2-one hydrazone dihydrate

Base Information

• Chemical Name: (2E)-azepan-2-one hydrazone dihydrate
• CAS No.: 31030-25-8
• Molecular Formula: C6H13 N3
• Molecular Weight: 127.189
• Hs Code.: 2933990090
• Mol file: 31030-25-8.mol

Synonyms:2H-Azepin-2-one,hexahydro-, hydrazone (9CI); 2H-Azepine, 7-hydrazino-3,4,5,6-tetrahydro-(6CI,8CI); 2-Hydrazino-1-aza-1-cycloheptene;7-Hydrazino-3,4,5,6-tetrahydro-2H-azepine

Chemical Property of (2E)-azepan-2-one hydrazone dihydrate

Chemical Property:

• Melting Point: 112 °C
• Boiling Point: 234.5±23.0 °C(Predicted)
• PKA: 9.36±0.20(Predicted)
• PSA: 68.87000
• Density: 1.19±0.1 g/cm3(Predicted)
• LogP: 1.32270

Purity/Quality:

99% ^*data from raw suppliers

(2E)-AZEPAN-2-ONE HYDRAZONE DIHYDRATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2E)-azepan-2-one hydrazone dihydrate

There total 5 articles about (2E)-azepan-2-one hydrazone dihydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O-methylcaprolactim (2525-16-8) → Caprolactimhydrazid (31030-25-8)

Guidance literature:

With hydrazine hydrate; In ethanol;

Reference yield:

O-methylcaprolactim (2525-16-8) → hexahydro-azepin-2-one-hydrazone (31030-25-8)

Guidance literature:

With hydrazine hydrate;

DOI:10.1021/ja01186a035

Reference yield:

caprolactam (105-60-2,9012-16-2) → hexahydro-azepin-2-one-hydrazone (31030-25-8)

Guidance literature:

Multi-step reaction with 2 steps

2: hydrazine hydrate

With hydrazine hydrate;

DOI:10.1021/ja01186a035

upstream raw materials:

O-methylcaprolactim

hydrazinium monoacetate

7-ethoxy-3,4,5,6-tetrahydro-2H-azepine

caprolactam

Downstream raw materials:

pentetrazole