(1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Base Information

• Chemical Name: (1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione
• CAS No.: 959911-16-1
• Molecular Formula: C₂₂H₃₄N₂O₄Si
• Molecular Weight: 418.608

Synonyms:(1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Chemical Property of (1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

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Technology Process of (1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

There total 1 articles about (1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

chloro-trimethyl-silane (75-77-4) + methyl (S)-3-(1-benzyl-4-butyl-3,6-dioxopiperazin-2-yl)propionate (433285-20-2) → (1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (959911-16-1)

Guidance literature:

methyl (S)-3-(1-benzyl-4-butyl-3,6-dioxopiperazin-2-yl)propionate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃; for 3.25h; Further stages.;

DOI:10.1016/j.ejmech.2007.02.005

Reference yield:

(1S,2R,5S)-6-benzyl-8-butyl-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (959911-16-1) → (1S,5S)-6-benzyl-8-butyl-6,8-diazabicyclo[3.2.2]nonane-2,7,9-trione (959911-17-2)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; water; at 20 ℃; for 16h;

DOI:10.1016/j.ejmech.2007.02.005

upstream raw materials:

chloro-trimethyl-silane

methyl (S)-3-(1-benzyl-4-butyl-3,6-dioxopiperazin-2-yl)propionate

Downstream raw materials:

(1S,5S)-6-benzyl-8-butyl-6,8-diazabicyclo[3.2.2]nonane-2,7,9-trione

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