Technology Process of C21H23I2NO6
There total 5 articles about C21H23I2NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / water / 24 h / 20 °C
2: sodium hydrogencarbonate / water; tetrahydrofuran / 24 h / 20 °C
3: N-iodo-succinimide / dichloromethane / 0.67 h / 0 °C
4: N-ethyl-N,N-diisopropylamine; pyridine; copper diacetate / dichloromethane / 48 h / 20 °C / Molecular sieve
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C
With
pyridine; hydrogenchloride; N-iodo-succinimide; tetrabutyl ammonium fluoride; copper diacetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1080/00397911.2011.639005
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogencarbonate / water; tetrahydrofuran / 24 h / 20 °C
2: N-iodo-succinimide / dichloromethane / 0.67 h / 0 °C
3: N-ethyl-N,N-diisopropylamine; pyridine; copper diacetate / dichloromethane / 48 h / 20 °C / Molecular sieve
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C
With
pyridine; N-iodo-succinimide; tetrabutyl ammonium fluoride; copper diacetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1080/00397911.2011.639005
