{Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

Base Information

• Chemical Name: {Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester
• CAS No.: 215511-60-7
• Molecular Formula: C₂₃H₂₀N₄O₆
• Molecular Weight: 448.435

Synonyms:{Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

Chemical Property of {Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

Chemical Property:

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Technology Process of {Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

There total 3 articles about {Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{Isopropylsulfanyl-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester (215511-57-2) → {Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester (215511-60-7)

Guidance literature:

With ammonia; mercury dichloride; In tetrahydrofuran; at 0 ℃; for 3h; Yield given;

DOI:10.1016/S0223-5234(98)80048-2

Reference yield:

2-amino-3'-nitro-benzophenone (3882-50-6) → {Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester (215511-60-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) N-methylmorpholine, iBuOCOCl / 1) CH₂Cl₂, 0 deg C, 15 min, 2) CH₂Cl₂, reflux, 20 min, r.t., overnight

2: NH₃, HgCl₂ / tetrahydrofuran / 3 h / 0 °C

With 4-methyl-morpholine; ammonia; mercury dichloride; isobutyl chloroformate; In tetrahydrofuran;

DOI:10.1016/S0223-5234(98)80048-2

Reference yield:

α-(Isopropylthio)-Nα-(benzyloxycarbonyl)glycine (103711-22-4) → {Amino-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester (215511-60-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) N-methylmorpholine, iBuOCOCl / 1) CH₂Cl₂, 0 deg C, 15 min, 2) CH₂Cl₂, reflux, 20 min, r.t., overnight

2: NH₃, HgCl₂ / tetrahydrofuran / 3 h / 0 °C

With 4-methyl-morpholine; ammonia; mercury dichloride; isobutyl chloroformate; In tetrahydrofuran;

DOI:10.1016/S0223-5234(98)80048-2

upstream raw materials:

{Isopropylsulfanyl-[2-(3-nitro-benzoyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

2-amino-3'-nitro-benzophenone

α-(Isopropylthio)-Nα-(benzyloxycarbonyl)glycine

Downstream raw materials:

[5-[3-(Imidazolidin-2-ylideneamino)-phenyl]-2-oxo-3-(quinoline-8-sulfonylamino)-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-acetic acid tert-butyl ester

[5-(3-Isocyano-phenyl)-2-oxo-3-(quinoline-8-sulfonylamino)-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-acetic acid tert-butyl ester

C₃₁H₂₇Br₂N₅O₅S

[5-(3-Nitro-phenyl)-2-oxo-3-(quinoline-8-sulfonylamino)-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-acetic acid tert-butyl ester

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