Technology Process of C7H7BrFNO
There total 4 articles about C7H7BrFNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C7H5BrFNO;
With
hydrogenchloride; methyl orange; sodium cyanoborohydride;
In
tetrahydrofuran; methanol; water;
for 16h;
pH=2;
With
potassium hydroxide;
In
tetrahydrofuran; methanol; water;
pH=7;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9
2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
2.2: pH 7
With
hydrogenchloride; potassium hydroxide; hydroxylamine hydrochloride; methyl orange; sodium cyanoborohydride;
In
tetrahydrofuran; methanol; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12.08 h
1.2: 2 h
2.1: pyridinium chlorochromate / dichloromethane / 1.08 h / Molecular sieve
3.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9
4.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
4.2: pH 7
With
hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; methyl orange; sodium cyanoborohydride; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane; water;
