C₂₉H₃₆N₂O₅

Base Information

Chemical Name:C₂₉H₃₆N₂O₅
CAS No.:132143-03-4
Molecular Formula:C₂₉H₃₆N₂O₅
Molecular Weight:492.615
Hs Code.:

C<sub>29</sub>H<sub>36</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₉H₃₆N₂O₅

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Chemical Property of C₂₉H₃₆N₂O₅

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Technology Process of C₂₉H₃₆N₂O₅

There total 15 articles about C₂₉H₃₆N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 132143-02-3
C₂₇H₃₀N₂O₄

: 149-73-5
trimethyl orthoformate

: 132143-03-4
C₂₉H₃₆N₂O₅

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 3h; Heating;
DOI:10.1016/S0040-4020(01)90540-X

Reference yield:

: 58594-50-6
3-(2'-nitrophenyl)pyrrolidine-2,5-dione

: 132143-03-4
C₂₉H₃₆N₂O₅

Guidance literature:: Multi-step reaction with 12 steps

1: Et₃N / DMAP / CH₂Cl₂ / 0 deg C to room temperature

2: 95 percent / H₂ / 10percent Pd/C / toluene; ethanol / 18 h / 760 Torr

3: toluene / Ambient temperature

4: 1.5 M n-BuLi / 2-methyl-propan-2-ol; tetrahydrofuran; hexane; toluene / 0.5 h / 5 °C

5: toluene

6: 20percent aq. HCl / ethanol / Ambient temperature

7: 98 percent / dimethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

8: 54 percent / NaBH₄, 2 N H₂SO₄ / ethanol / 0 °C

9: 1.) Et₃N, MeSO₂Cl / 1.) THF, -30 deg C to room temperature, 15 min, 2.) 90 min

10: 69 percent / BF₃*Et₂O, CaH₂ / CH₂Cl₂ / 60 h

11: 1.) ozone, 2.) dimethyl sulfide / 1.) CH₂Cl₂, - 78 deg C, 2.) -78 deg C to room temperature, 2 h

12: 79 percent / p-toluenesulfonic acid monohydrate / methanol / 3 h / Heating

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; calcium hydride; dimethylsulfide; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; toluene-4-sulfonic acid; ozone; methanesulfonyl chloride; dimethyl azodicarboxylate; triethylamine; triphenylphosphine; dmap; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)90540-X

Reference yield:

: 132143-08-9
1-(tert-Butyl-dimethyl-silanyl)-3-(2-nitro-phenyl)-pyrrolidine-2,5-dione

: 132143-03-4
C₂₉H₃₆N₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1: 95 percent / H₂ / 10percent Pd/C / toluene; ethanol / 18 h / 760 Torr

2: toluene / Ambient temperature

3: 1.5 M n-BuLi / 2-methyl-propan-2-ol; tetrahydrofuran; hexane; toluene / 0.5 h / 5 °C

4: toluene

5: 20percent aq. HCl / ethanol / Ambient temperature

6: 98 percent / dimethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

7: 54 percent / NaBH₄, 2 N H₂SO₄ / ethanol / 0 °C

8: 1.) Et₃N, MeSO₂Cl / 1.) THF, -30 deg C to room temperature, 15 min, 2.) 90 min

9: 69 percent / BF₃*Et₂O, CaH₂ / CH₂Cl₂ / 60 h

10: 1.) ozone, 2.) dimethyl sulfide / 1.) CH₂Cl₂, - 78 deg C, 2.) -78 deg C to room temperature, 2 h

11: 79 percent / p-toluenesulfonic acid monohydrate / methanol / 3 h / Heating

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; calcium hydride; dimethylsulfide; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; toluene-4-sulfonic acid; ozone; methanesulfonyl chloride; dimethyl azodicarboxylate; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)90540-X