Technology Process of (4-hydroxy-3-iodophenyl)(3-iodophenyl)methanone
There total 4 articles about (4-hydroxy-3-iodophenyl)(3-iodophenyl)methanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(4-hydroxyphenyl)(3-iodophenyl)methanone;
With
potassium iodide;
at 25 ℃;
for 0.25h;
Inert atmosphere;
Schlenk technique;
With
iodine; potassium iodide;
In
water;
at 25 ℃;
for 14h;
Inert atmosphere;
Schlenk technique;
DOI:10.1039/c3ra46392c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / dichloromethane / 0.17 h / 0 - 10 °C / Inert atmosphere; Schlenk technique
1.2: 10 - 20 °C / Inert atmosphere; Schlenk technique
2.1: hydrogen bromide; acetic acid / 24 h / Inert atmosphere; Schlenk technique; Reflux
3.1: potassium iodide / 0.25 h / 25 °C / Inert atmosphere; Schlenk technique
3.2: 14 h / 25 °C / Inert atmosphere; Schlenk technique
With
aluminum (III) chloride; hydrogen bromide; acetic acid; potassium iodide;
In
dichloromethane;
1.1: |Friedel-Crafts Acylation;
DOI:10.1039/c3ra46392c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / dichloromethane / 0.17 h / 0 - 10 °C / Inert atmosphere; Schlenk technique
1.2: 10 - 20 °C / Inert atmosphere; Schlenk technique
2.1: hydrogen bromide; acetic acid / 24 h / Inert atmosphere; Schlenk technique; Reflux
3.1: potassium iodide / 0.25 h / 25 °C / Inert atmosphere; Schlenk technique
3.2: 14 h / 25 °C / Inert atmosphere; Schlenk technique
With
aluminum (III) chloride; hydrogen bromide; acetic acid; potassium iodide;
In
dichloromethane;
1.1: |Friedel-Crafts Acylation;
DOI:10.1039/c3ra46392c
